shaking le can clean antimony

Details of the ICP-MS parameters used during Sb and Br determination can be found in the Supporting information (Table SI-1). Total soluble Sb and Br was defined as the freely available and labile forms of antimony and bromine in bottled water, irrespective of species/speciation forms, after thorough mixing by hand shaking on the day of sampling.

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The first part begins with adding 5.0mL of antimony trichloride solution to a clean 75mL test tube. Four 4.0mL increments of distilled water are added to the test tube, the appearance of the solution is recorded each time, before and after shaking.

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